MIT-IVY Athena best hot seller N,N-DIMETHYL-P-TOLUIDINE Factory CAS 99-97-8 china in stock factory best top 1 whatsapp:008613805212761
Quick Details
CAS No. |
99-97-8 |
Other Names |
N,N,4-Trimethylaniline |
MF |
C9H13N |
Place of Origin |
xuzhou, China |
Type |
Pharmaceutical Intermediates |
Purity |
99% |
Brand Name |
mit-ivy |
Appearance |
light yellow liquid |
Product name |
n,n-dimethyl-p-toluidin |
Shipping methods: |
By Courier, by air or by sea |
Density |
0.937 g/mL at 25 °C(lit.) |
Color |
light yellow liquid |
Molecular Weight |
135.21 |
Boiling point |
211 °C(lit.) |
Assay |
99% |
Molecular formula |
C9H13N |
Flash point |
182 °F |
EINECS |
202-805-4 |
Packing and storage of N,N-DiMethyl-p-toluidine
N,N-DiMethyl-p-toluidine is normally packed in 200KG Iron Drums.
Store in cool and dry place, away from sun light.
Specification List
Item | Specifications | Results |
Identification (By GC) | Conform to the standard | Conform to the standard |
Appearance | Primrose yellow liquid | Qualitied |
N,N-dimethyl-p-toluidine assay | ≥99.00% | 99.22% |
p-toluidine assay | ≤0.05% | 0.03% |
N-methyl-p-toluidine assay | 0.70% | 0.53% |
Another assay | 0.30% | 0.22% |
Conclusion | The results conforms with enterprise standards |
Specification:
Appearance |
White to flavescent powder |
Purity (%) |
≥96 |
Total colorless dye (%) |
≥97 |
Color intensity (%) |
≥97 (as compared with reference standard) |
Diarylethane insolube substances (%) |
≤0.2 |
mp (°C) |
≥178 |
Volatile substances (%) |
≤0.1 |
Safety information on dangerous goods
Mark:T Hazard Class Number:23/24/25-33-52/53Safety Instructions:28-36/37-45-61-28A-51-44-36-22-20/21Dangerous Goods Transport Number:1708WGKGermany:3RTECS Number:XU5803000F:8-10-23Self-ignition temperature:425° CTSCA:YesCustoms Code:29214300HazardClass:6.1PackingGroup:IIToxicity:LD50orallyinRabbit:1650mg/kgN,N-Dimethyl-p-toluidineProperties,Uses and Production ProcessPhysical and Chemical PropertiesN,N-Dimethyl-p-toluidine is a colorless or light yellow oily substance. Liquid, with rotten egg smell, melting point 130.31℃, boiling point 211.5-212.5℃, weight 0.9287-0.Chemicalbook9366g/mL at room temperature, refractive index 1.5360-1.5470, insoluble in water, soluble in some organic solvents, decomposed by light. It is used as an effective photoinitiator for the polymerization of acrylonitrile (AN), and its polymerization speed is proportional to the 1.62nd of AN concentration and the 0.62nd of DMT concentration. The product is commonly used as a promoter, and in addition it is used as an additive in the synthesis of unsaturated polyesters, bonding agents, etc. Synthesis method: N,N-dimethyl-p-toluidine is synthesized by using dimethyl sulfate as a methylating agent at low temperature and atmospheric pressure. N,4-Dimethyl-N-(3-phenylprop-2-ynyl)benzylamine and N-(methyl(p-tolyl)amino)methyl)benzamide are formed by iron-catalyzed oxidative C-C coupling with phenacetylene and benzamide in the presence of di-tert-butyl peroxide, respectively.
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